Maintaining a proper electroless nickel solution within its plating bath chemistry begins. Our scientifically developed methodology, backed by more than 80 years of metal finishing experience, includes a finely honed preplating process to improve longevity and eliminate. Precision process equipment equipment continuous plating. Oct 08, 2010 this is my attempt at making a tin sulfate electroplating solution from scratch. Electrochemical aspects of tin electrodeposition on copper. The allover plating cell is designed for the continuous plating of strip material, preformed connectors, lead frames, and other formed or stamped components. If the coating or plating is uneven or not the correct thickness, usually microscopy analysis of sample crosssections can quantify the coating dimensions and variance. Making tin sulfate solution for pcb electroplating youtube. Solution analysis the management of plating bath components, including both primary components and trace components and additives, is critical to quality and cost control.
An external solution reservoir with heater, filtration system and transfer pump provide fresh, high metal content plating solution to the strip material. Grain structure of galvanic tin coatings obtained with di. The technic rta real time analyzer has set the standard for robust analytical performance in plating for over a decade. Iron and copper analysis iron and copper, as well as other heavy metal contaminants, are analyzed using an atomic absorption emission spectrophotometer operated in the absorption mode. Our company can also certify tin plating services to iso 2093 as well as most companyspecific tin plating specifications. Software simulates electroplating products finishing. Us10072347b2 systems and methods for tin antimony plating. The plating process is multifaceted and in some cases extremely complex. Twl blue rhodium bath plating solution 1 gram in 500ml. The two most common tin plating services certified by advanced plating technologies are milt10727, astm b545 and ams 2408. Elsyca platingmaster predicts current density and deposited layer thickness distributions for both decorative and functional plating applications. Oct 14, 2012 the electrolyte solution is made by dissolving tin into the acid. With measurement devices from fischer you can, for example, non destructively analyze coatings made from chemical nickel or crnicu within the.
The package, a customized user interface cui, provides a userfriendly interface that allows users with only limited training to build a fea model of their parts. Electroplating lab facility for quality control at klein plating works, inc. However, it is expensive, prone to tin whiskers due to the high sn content. The colgleam sn process is extremely simple to control, requiring only a fraction of the lab and analysis time. With over 100 installations, anoplex software is the leading supplier of software to the metal finishing industry.
Control and chemical analysis of plating solutions. Copper in this form is well tolerated by most immersion tin plating baths, and at reasonable levels has no effect. Before the first production run takes place, elsyca platingmaster. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed. First, the specialized cell is filled with the solution to be analyzed, then it is covered with a thin but robust mylar foil and sealed with a plastic ring all part of the solution analysis kit. Technics electroplating bath analyzer eba offers manufacturers an easy to implement, accurate and troublefree analysis of electroplating bath solutions. Sep 01, 2008 however, looking at the plating process as a whole, there are a multitude of other factors that go into controlling the process in addition to just solution analysis.
Elsyca platingmaster is a cadbased simulation software platform for the analysis and optimization of electroplating processes. Elsyca platingmaster elsyca nv electrochemical modelling. In order to facilitate this,a standard operating procedure should be documented, and adequate records with tank id, date and time of analysis, and any additions made for replenishment should be maintained, preferably using commercial software. You can just sit back and watch as we work remotely on your equipment. Tin electroplating kits tin plating kits plating kits. Degrease your parts and hang them into the solution from string or copper wire. Jobpro routers identify the buyoffs and data entry required by ac7108, and jobpad allows all the data to be collected in a. Simulations are executed using a virtual mockup of your inhouse plating line and detailed layer thickness and quality results are available for every part on the rack and for every plating. Tin deposits are widely used in foodstuff processing and canning materials because it is a non toxic, ductile and corrosion resistant metal 1, 2. To me, the only way to get a high quality consistent product is to start with an excellent bath formula and then use exacting amounts of pure chemicals and. We offer a plating deposit as a leadfree solder for hightemperature connections, and as a solder for highstrength and highreliability connections. Electrochemical aspects of tin electrodeposition on copper in. This is my attempt at making a tin sulfate electroplating solution from scratch. The information in this msds is, to the best of our knowledge, believed to be accurate.
First, we do a complete analysis of your needs free to determine which mix of software and services you need. The chemical analysis of plating solutions that must be analyzed to maintain the recommended bath formulation and to preempt the occurrence of problems related to. All the fischer xrf instruments can be easily outfitted for analysing plating solutions by mounting the optional solution analysis cell see figure 2. Ideal for model tinware trains, antique tinware, cooking utensils, electronics, buss bars, tools and much more tin is a very commonly used metal for the protection of steel. Tin plating services electroplating milt10727, astm b545. This highly reliable design offers a troublefree and accurate analysis of your electroplating soluti.
It is used extensively in the food trade because of its nontoxic qualities. Onsite analytical lab for metal plating analytical lab. We can provide a thinner plating deposit than sheet material or ribbon material. Immerse in the 120f solution for 60 seconds to put a bright tin plating onto the base metal. Quality control of the tin or tinlead electroplating solutions is critical to meet. Chemical analysis of plating solutions request pdf. Control of tinlead solutions for electrodeposition of bumps eci.
The chemical analysis of plating solutions that must be analyzed to maintain the recommended bath formulation and to preempt the occurrence of problems related to improper levels of bath constituents. Ideal for model tin ware trains, antique tin ware, cooking utensils, electronics, buss bars, tools and much more tin is a very commonly used metal for the protection of steel. Electroless tin plating kit tin plate copper, brass, gold and copper based alloys without power or heat. Required for professional prototyping process and the electroplating process. As shown, the tin electrode is moved around the plating target during the electroplating process to provide a more uniform plating. Spc is widely recognized as an industry leader in the development of topquality tin plating processes that also offer a costeffective metal finishing solution. Tin is widely used in the electronics industry because of its ability to protect the base metal from oxidation. The technic analytical controls group designed the eba to utilize a patented combination of processing techniques, software and hardware that achieve greater. Effect of additives on electrodeposition of tin and its. Printed circuit board fabrication immersion tinfinal finish. It didnt turn out the way i wanted, and the solution looks like. It is the electrochemical process whereby metal ions in solution are bonded to a metal substrate via electrodeposition. Full text of electroplating and analysis of solutions.
Kpw employs a fulltime staff of highly knowledgeable personnel dedicated to analyzing and maintaining all of its processes in its inhouse laboratory. The electrolyte solution is made by dissolving tin into the acid. Advanced plating technologies is excited to bring yet another engineered solution in metal finishing. Since electroplating involves both an electrical and a chemical reaction at the surface of the part, exposure to the plating chemistry is critical to the overall performance of the finished product.
The technic analytical controls group designed the eba to utilize a patented combination of processing techniques, software and hardware that achieve greater consistency and accuracy in. Because the 2 mol tin is is what i would like to maintain, is it possible to convert the 4 and 10 molecule tin back to 2 and still keep the integrity of the plating solution. Modern electroplating is a form of metal finishing used in various industries, including aerospace, automotive, military, medical, rf microwave, space, electronics and battery manufacturing. Then the bus bar is placed in a diluted solution and a 1 a current is run through it. Xrf is useful in measuring the major constituents of plating baths such as cadmium, chromium, cobalt, gold, nickel, silver, tin, and zinc. Etching and tin plating hydrochloric acid, hydrogen peroxide, liquid tin duration.
Iron and copper analysis iron and copper, as well as other heavy metal contaminants, are analyzed using an atomic absorption emission spectrophotometer operated. Bowman xrf technology provides a highprecision, nondestructive, fast and user friendly way to analyze the metallic content of plating solutions. Elsyca platingmanager software electroplating simulation. Potentiometric analysis of tin plating baths metrohm ag.
Real time analyzer rta for process control technic inc. The container is a generic large plastic bin and the plating process took place in a well ventilated environment, as hydrogen gas and potentially small amounts of chlorine gas is generated in the process. Simulations are executed using a virtual mockup of your inhouse plating line and detailed layer thickness and quality results are available for every part on the rack and for every plating step. Electroplating lab quality control klein plating works. Electroless nickel plating gold plating silver plating copper plating tin plating nickel. Analysis of plating baths using the icap 7400 icpoes. Tin plating systems whether a standard tin technology is what you require or a high technology tin alloy, pavco provides the correct solution to meet your needs.
Corrosion behavior of tinplated carbon steel and aluminum. When tin immersion plates on to the copper, two atoms of copper dissolve for every atom of tin that plates out. However, looking at the plating process as a whole, there are a multitude of other factors that go into controlling the process in addition to just solution analysis. Most electroplating systems require the user to mix four or more chemicals to create a plating solution. Plates tin over copper, brass, gold and copper based alloys in seconds.
Bluestreak plating software throughput consulting inc. Electroless tin plating kits tin plating kits plating. Tin electroplating solution 41672 recommended for use with mg chemicals electroplating tank cat. Diy chemical tin plating that really works fast youtube. Elsyca platingmanager is the stateoftheart graphical simulation platform for analyzing the production performance and quality of electroplating processes. I am trying to find methods of analysis of a tin plating bath solution which consists of. Tin plating services industrial tin plating services. Instructions for kepros immersion tin plating solution itp. Dear sirs, i am trying to find methods of analysis of a tin plating bath solution which consists of. Chemical analysis of plating solutions in pdf format clarkson. Both rack plating and barrel plating are available. Our scientifically developed methodology, backed by more than 80 years of metal finishing experience, includes a finely honed pre plating process to improve longevity and eliminate. Tin plating services electroplating milt10727, astm. Besides the right color, the main thing required is a consistent product.
Analysis of plating baths using the thermo scientific icap 7400 icpoes application note 43150 authors nora bartsch, application specialist, thermo fisher scientific, bremen, germany keywords method of standard addition, plating baths, sulphuric acid levels introduction the plating of metal is an ancient technique, used for hundreds of years. Tin plating ensures solderability of the base metal, a critical requirement when. Active, expires 203403 application number us646,401 other versions us20140209468a1 en. It didnt turn out the way i wanted, and the solution looks like crap. The analytical methods for analysis ofplating solutions should besimple, direct, andoperatorfriendly. This rhodium solution specifically formulated for bath plating.
Nesting of parts will result in a lack of adhesion or coverage on the. Tin is a bright, shiny material, and has excellent soldering capabilities, making it ideal for all electrical connection applications. Ens technology is the only metal plating company in northern california to maintain a. The analysis will vary depending on the type of coating or plating problem. Technics eba electroplating bath analyzer provides an easy to implement, accurate and troublefree analysis of electroplating solutions. Making a plating solution for your own use is one thing but making a solution to sell is a totally different deal.
Potentiometric titration methods for the analysis of acid and alkaline tin plating baths are presented. The technic rta real time analyzer has set the standard for robust analytical performance in plating for. Ens technology is the only metal plating company in northern california to maintain a fully equipped, onsite analytical laboratory. Baths are maintained with only one brightener additive, eliminating the need to juggle and balance brighteners. For more information on our full line of tin technologies, please contact a pavco technical service representative here or browse below to learn more about our products. Then, we remotely install, configure and setup the systems. In contrast, there was little incremental change in the corrosion rates of aluminum when the nacl concentration was increased from 1. Using the right analytics solution can help electroplating and coating manufacturers ensure product quality, optimize production processes to support water. The company says its finiteelement analysis software for plating simulation produces accurate coating uniformity in electroplating with no specialized training required. Proprietary software that allows for 24hour monitoring anywhere in the world. Tin and its alloys are used in the industry for different purposes, such as corrosion protection, metal finishing and improvement of weld strength in certain dissimilar joints, among others.
The electrodeposition of tin is an electrochemical process employed since long time ago for a wide spectrum of applications. This msds was prepared in accordance with the requirements of the osha hazard communication standard 29 cfr 1910. Instructions for kepros immersion tin plating solution. Na2sno3 3h2o 70 grl, naoh 11 grl,and lch3coona22 grl. Jobpro is the only job system designed for nadcap accredited companies. This highly reliable design offers a troublefree and accurate analysis of your electroplating solutions. What an engineer or designer should consider before electroplating. The plating solution is made up of nickel chloride, stannous chloride anhydrous, ammonium bifluoride, ammonium hydroxide, and d. Nesting of parts during the electroplating process. Hach water monitoring and analysis solutions for electroplating. These include the cleaning cycles, racking techniques, rinsing techniques, filtration, equipment preventive maintenance and part testing, among many other items.